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This test work is based on game plan ofshape-memory Nano composite using high energy ball plant .Preciseballtopowderproportion, working medium, and ballmill speed are cardinalfactors which choose effectively ofmilling movement. In presentwork select material is small sizepowder Zn, Cu, and Al of chosen degree. In beginning step powder was dissipate handled to 24hours and tests were taken for X-bar diffraction, scanningelectron microscopy, differential analyzing calorimetric analysis.In presence of liquid nitrogen handling time certainly reducedwith fineparticlesizereduction andfeature.Togetrequiredcharacteristics,controlofparticlesizeisthemostcrucialphasein action. Alloying by HEBM is an imaginative technique, thistechnique work with palatable and strong control overchangesatgrainboundarylevelandexternalmorphologybyprecisecontrolovermillingvariables.